Basic Gas Chromatography

by ;
Format: Hardcover
Pub. Date: 1997-10-01
Publisher(s): Wiley-Interscience
  • Free Shipping Icon

    This Item Qualifies for Free Shipping!*

    *Excludes marketplace orders.

List Price: $79.95

Buy New

Usually Ships in 3-4 Business Days
$79.87

Rent Textbook

Select for Price
There was a problem. Please try again later.

Used Textbook

We're Sorry
Sold Out

eTextbook

We're Sorry
Not Available

How Marketplace Works:

  • This item is offered by an independent seller and not shipped from our warehouse
  • Item details like edition and cover design may differ from our description; see seller's comments before ordering.
  • Sellers much confirm and ship within two business days; otherwise, the order will be cancelled and refunded.
  • Marketplace purchases cannot be returned to eCampus.com. Contact the seller directly for inquiries; if no response within two days, contact customer service.
  • Additional shipping costs apply to Marketplace purchases. Review shipping costs at checkout.

Summary

Gas Chromatography (GC) is undoubtedly the most widely used technique for the separation and analysis of volatile compounds. Yet comprehensive guides to contemporary GC theory and practice are surprisingly hard to find. Basic Gas Chromatography fills this significant void in the GC literature. Written by two well-known practitioners and educators in GC, it offers thorough coverage of the basic principles and techniques of modern gas chromatography. Designed to serve as a primer/working reference for bench chemists and as a textbook for upper-level undergraduate and graduate students, it presents the fundamentals in a straightforward and logical fashion. Theoretical issues are explained without complicated equations and derivations and always in terms of how they relate to practical operating principles. Timely, comprehensive, and accessible, Basic Gas Chromatography: Provides a balanced presentation of theory and practice Includes both capillary column and packed column chromatography Uses the new IUPAC terms throughout, cross-referenced to traditional terms and symbols Offers a wealth of helpful hints, step-by-step guidelines, and trouble-shooting tips Briefly covers GC-MS, headspace analysis, chiral analysis, solid phase microextraction, and other cutting-edge topics.

Table of Contents

Series Preface ix(2)
Preface xi
1 Introduction
1(13)
A Brief History
1(2)
Definitions
3(6)
Overview: Advantages and Disadvantages
9(3)
Instrumentation
12(2)
2 Instrument Overview
14(15)
Carrier Gas
15(2)
Flow Control and Measurement
17(3)
Sample Inlets and Sampling Devices
20(4)
Columns
24(1)
Temperature Zones
25(2)
Detectors
27(1)
Data Systems
27(2)
3 Basic Concepts and Terms
29(26)
Definitions, Terms, and Symbols
29(11)
The Rate Theory
40(11)
A Redefinition of H
51(1)
The Achievement of Separation
52(3)
4 Stationary Phases
55(18)
Selecting a Column
55(1)
Classification of Stationary Phases for GLC
56(11)
Liquid Stationary Phases (GLC)
67(4)
Solid Stationary Phases (GSC)
71(2)
5 Packed Columns and Inlets
73(13)
Solid Supports
73(2)
Liquid Stationary Phases
75(1)
Solid Stationary Phases (GSC)
76(3)
Gas Analysis
79(3)
Inlets for Liquid Samples and Solutions
82(1)
Special Columns
83(1)
Upgrading for Capillary Columns
84(2)
6 Capillary Columns and Inlets
86(15)
Types of OT Columns
86(2)
OT Column Tubing
88(2)
Advantages of OT Columns
90(1)
Column Selection
91(6)
Capillary Inlet Systems
97(4)
7 Detectors
101(25)
Classification of Detectors
102(3)
Detector Characteristics
105(7)
Flame Ionization Detector (FID)
112(4)
Thermal Conductivity Detector (TCD)
116(3)
Electron Capture Detector (ECD)
119(4)
Other Detectors
123(3)
8 Qualitative and Quantitative Analysis
126(16)
Qualitative Analysis
126(5)
Quantitative Analysis
131(11)
9 Programmed Temperature
142(11)
Temperature Effects
142(2)
Advantages and Disadvantages of PTGC
144(2)
Requirements of PTGC
146(2)
Theory of PTGC
148(2)
Special Topics
150(3)
10 Special Topics
153(20)
GC-MS
153(10)
Chiral Analysis by GC
163(1)
Special Sampling Methods
164(2)
Derivatization
166(7)
11 Troubleshooting GC Systems
173(7)
Appendixes 180(13)
I. List of Symbols and Acronyms
180(3)
II. Guidelines for Selecting Capillary Columns
183(2)
III. GC: How to Avoid Problems
185(2)
IV. Calculation of Split Ratio for Split Injection on OT Columns
187(1)
V. Operating Conditions for Capillary Columns
187(1)
VI. OV Liquid Phases Physical Property Data
188(2)
VII. Some Pressure Correction Factors (j)
190(1)
VIII. List of Some Chromatographic Supply Houses
191(1)
IX. Other Resources
192(1)
Index of Applications 193(1)
Index 194

An electronic version of this book is available through VitalSource.

This book is viewable on PC, Mac, iPhone, iPad, iPod Touch, and most smartphones.

By purchasing, you will be able to view this book online, as well as download it, for the chosen number of days.

Digital License

You are licensing a digital product for a set duration. Durations are set forth in the product description, with "Lifetime" typically meaning five (5) years of online access and permanent download to a supported device. All licenses are non-transferable.

More details can be found here.

A downloadable version of this book is available through the eCampus Reader or compatible Adobe readers.

Applications are available on iOS, Android, PC, Mac, and Windows Mobile platforms.

Please view the compatibility matrix prior to purchase.