Series Preface |
|
ix | (2) |
Preface |
|
xi | |
|
|
1 | (13) |
|
|
1 | (2) |
|
|
3 | (6) |
|
Overview: Advantages and Disadvantages |
|
|
9 | (3) |
|
|
12 | (2) |
|
|
14 | (15) |
|
|
15 | (2) |
|
Flow Control and Measurement |
|
|
17 | (3) |
|
Sample Inlets and Sampling Devices |
|
|
20 | (4) |
|
|
24 | (1) |
|
|
25 | (2) |
|
|
27 | (1) |
|
|
27 | (2) |
|
3 Basic Concepts and Terms |
|
|
29 | (26) |
|
Definitions, Terms, and Symbols |
|
|
29 | (11) |
|
|
40 | (11) |
|
|
51 | (1) |
|
The Achievement of Separation |
|
|
52 | (3) |
|
|
55 | (18) |
|
|
55 | (1) |
|
Classification of Stationary Phases for GLC |
|
|
56 | (11) |
|
Liquid Stationary Phases (GLC) |
|
|
67 | (4) |
|
Solid Stationary Phases (GSC) |
|
|
71 | (2) |
|
5 Packed Columns and Inlets |
|
|
73 | (13) |
|
|
73 | (2) |
|
|
75 | (1) |
|
Solid Stationary Phases (GSC) |
|
|
76 | (3) |
|
|
79 | (3) |
|
Inlets for Liquid Samples and Solutions |
|
|
82 | (1) |
|
|
83 | (1) |
|
Upgrading for Capillary Columns |
|
|
84 | (2) |
|
6 Capillary Columns and Inlets |
|
|
86 | (15) |
|
|
86 | (2) |
|
|
88 | (2) |
|
|
90 | (1) |
|
|
91 | (6) |
|
|
97 | (4) |
|
|
101 | (25) |
|
Classification of Detectors |
|
|
102 | (3) |
|
|
105 | (7) |
|
Flame Ionization Detector (FID) |
|
|
112 | (4) |
|
Thermal Conductivity Detector (TCD) |
|
|
116 | (3) |
|
Electron Capture Detector (ECD) |
|
|
119 | (4) |
|
|
123 | (3) |
|
8 Qualitative and Quantitative Analysis |
|
|
126 | (16) |
|
|
126 | (5) |
|
|
131 | (11) |
|
|
142 | (11) |
|
|
142 | (2) |
|
Advantages and Disadvantages of PTGC |
|
|
144 | (2) |
|
|
146 | (2) |
|
|
148 | (2) |
|
|
150 | (3) |
|
|
153 | (20) |
|
|
153 | (10) |
|
|
163 | (1) |
|
|
164 | (2) |
|
|
166 | (7) |
|
11 Troubleshooting GC Systems |
|
|
173 | (7) |
Appendixes |
|
180 | (13) |
|
I. List of Symbols and Acronyms |
|
|
180 | (3) |
|
II. Guidelines for Selecting Capillary Columns |
|
|
183 | (2) |
|
III. GC: How to Avoid Problems |
|
|
185 | (2) |
|
IV. Calculation of Split Ratio for Split Injection on OT Columns |
|
|
187 | (1) |
|
V. Operating Conditions for Capillary Columns |
|
|
187 | (1) |
|
VI. OV Liquid Phases Physical Property Data |
|
|
188 | (2) |
|
VII. Some Pressure Correction Factors (j) |
|
|
190 | (1) |
|
VIII. List of Some Chromatographic Supply Houses |
|
|
191 | (1) |
|
|
192 | (1) |
Index of Applications |
|
193 | (1) |
Index |
|
194 | |